ChemicalBook >> CAS DataBase List >>1,4-Cyclohexanedione bis(ethylene ketal)

1,4-Cyclohexanedione bis(ethylene ketal)

CAS No.
183-97-1
Chemical Name:
1,4-Cyclohexanedione bis(ethylene ketal)
Synonyms
1,4-Cyclohexanedione diethylene ketal;1,4-CYCLOHEXANEDIONE BIS(ETHYLENEKETAL);1,4-CYCLOHEXANEDIONE BISETHYLENE KETAL F;1,4-CYCLOHEXANEDIONE BIS(ETHYLENE ACETAL);1,4-Cyclohexianedione bis(ethylene acetal);1,4-Cyclohexanedione Bis(ethyleneketal) >1,4,9,12-TETRAOXADISPIRO[4.2.4.2]TETRADECANE;2,5-bis(butylamino)cyclohexa-2,5-diene-1,4-dione;1,4,9,12-tetraoxadispiro[4.2.4^{8}.2^{5}]tetradecane;Dispiro[1,3-dioxolane-2,1'-cyclohexane-4',2''-[1,3]dioxolane]
CBNumber:
CB1668030
Molecular Formula:
C10H16O4
Molecular Weight:
200.23
MDL Number:
MFCD00010851
MOL File:
183-97-1.mol
MSDS File:
SDS
Last updated:2023-11-27 16:18:02

1,4-Cyclohexanedione bis(ethylene ketal) Properties

Melting point 79-80 °C (lit.)
Boiling point 75-85 °C/0.5 mmHg (lit.)
Density 1.1508 (rough estimate)
refractive index 1.4459 (estimate)
Flash point 75-85°C/0.5mm
storage temp. Store below +30°C.
form powder to crystal
color White to Almost white
InChI InChI=1S/C10H16O4/c1-2-10(13-7-8-14-10)4-3-9(1)11-5-6-12-9/h1-8H2
InChIKey YSMVSEYPOBXSOK-UHFFFAOYSA-N
SMILES O1C2(CCC3(OCCO3)CC2)OCC1
CAS DataBase Reference 183-97-1(CAS DataBase Reference)
NIST Chemistry Reference 1,4-Cyclohexanedione bis(ethylene ketal)(183-97-1)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P264-P271-P280-P302+P352-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-37/39
WGK Germany  3
HS Code  29329990
NFPA 704
1
0 0

1,4-Cyclohexanedione bis(ethylene ketal) price More Price(12)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 298743 1,4-Cyclohexanedione bis(ethylene ketal) 99% 183-97-1 10g $96.8 2023-06-20 Buy
TCI Chemical C1544 1,4-Cyclohexanedione Bis(ethyleneketal) >99.0%(GC) 183-97-1 25g $65 2024-03-01 Buy
Alfa Aesar B20784 1,4-Cyclohexanedione bis(ethylene acetal), 99% 183-97-1 10g $40.65 2024-03-01 Buy
Alfa Aesar B20784 1,4-Cyclohexanedione bis(ethylene acetal), 99% 183-97-1 50g $118 2021-12-16 Buy
Alfa Aesar B20784 1,4-Cyclohexanedione bis(ethylene acetal), 99% 183-97-1 250g $467.65 2024-03-01 Buy
Product number Packaging Price Buy
298743 10g $96.8 Buy
C1544 25g $65 Buy
B20784 10g $40.65 Buy
B20784 50g $118 Buy
B20784 250g $467.65 Buy

1,4-Cyclohexanedione bis(ethylene ketal) Chemical Properties,Uses,Production

General Description

Hydrolysis of 1,4-cyclohexanedione bis(ethylene ketal) at 250°C has been reported.

Synthesis

After mixing 2243 g (20 mol) of 1,4-cyclohexanedione, 2607 g (42 mol) of ethylene glycol, the resin filtered, and 26 L of toluene, the temperature was raised slowly and refluxed for 11 hours to separate the water. The reaction temperature was lowered to 40° C., the resin was filtered, and the organic phase was concentrated until no liquid flowed. Then add 1257g (21mol) of methylboronic acid and 20L of n-heptane, raise the temperature to 80°C and react for 6 hours, then slowly cool down to 5-10°C in a gradient, filter, rinse the filter cake with n-heptane, and dry to obtain 1,4-Cyclohexanedione bis(ethylene ketal).
1,4-Cyclohexanedione bis(ethylene ketal)

1,4-Cyclohexanedione bis(ethylene ketal) Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 94)Suppliers
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Xi'an Tuochao Biotechnology Co., Ltd
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CONIER CHEM AND PHARMA LIMITED
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Hebei Guanlang Biotechnology Co., Ltd.
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GIHI CHEMICALS CO.,LIMITED
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Aladdin Scientific
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Amadis Chemical Company Limited
571-89925085 sales@amadischem.com China 131981 58
Mainchem Co., Ltd. +86-0592-6210733 sale@mainchem.com China 32360 55

View Lastest Price from 1,4-Cyclohexanedione bis(ethylene ketal) manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,4-Cyclohexanedione bis(ethylene ketal) pictures 2020-01-15 1,4-Cyclohexanedione bis(ethylene ketal)
183-97-1
US $5.50 / KG 1KG 98%min 1kg-100kg Career Henan Chemical Co
1,4-Cyclohexanedione diethylene ketal 1,4-Cyclohexianedione bis(ethylene acetal) Dispiro[1,3-dioxolane-2,1'-cyclohexane-4',2''-[1,3]dioxolane] 1,4-CYCLOHEXANEDIONE BISETHYLENE KETAL F 1,4,9,12-TETRAOXADISPIRO[4.2.4.2]TETRADECANE 1,4-CYCLOHEXANEDIONE BIS(ETHYLENE ACETAL) 1,4-CYCLOHEXANEDIONE BIS(ETHYLENEKETAL) 1,4,9,12-tetraoxadispiro[4.2.4^{8}.2^{5}]tetradecane 2,5-bis(butylamino)cyclohexa-2,5-diene-1,4-dione 1,4-Cyclohexanedione Bis(ethyleneketal) > 183-97-1 Dioxolanes Dioxanes & Dioxolanes Building Blocks Oxygen Compounds Organic Building Blocks Acetals/Ketals/Ortho Esters Dioxanes & Dioxolanes Dioxolanes Acetals/Ketals/Ortho Esters Building Blocks Chemical Synthesis Organic Building Blocks Oxygen Compounds