BENZENESULFINYL CHLORIDE

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Company Name: Shenzhen Nexconn Pharmatechs Ltd
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Products Intro: Product Name:BENZENESULFINYL CHLORIDE
CAS:4972-29-6
Purity:0.98 Package:1KG;10KG;50KG
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Products Intro: Product Name:BENZENESULFINYL CHLORIDE
CAS:4972-29-6
Purity:0.95 Package:500mg;1g;5g;10g;25g
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Products Intro: Product Name:Benzenesulfinic chloride
CAS:4972-29-6
Purity:98% Package:$185.9/1g;$645.9/5g;Bulk package Remarks:98%
Company Name: Beijing Taiya Jie Technology Development Co., Ltd.  
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Products Intro: Product Name:BENZENESULFINYL CHLORIDE
CAS:4972-29-6
Purity:97% GC Package:10g,50g,100g ,500g ,1Kg
Company Name: Bide Pharmatech Ltd.  
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Products Intro: Product Name:Benzenesulfinic chloride
CAS:4972-29-6
Purity:95% Package:250mg;1g;5g Remarks:BD00733391
BENZENESULFINYL CHLORIDE Basic information
Product Name:BENZENESULFINYL CHLORIDE
Synonyms:BENZENESULFINYL CHLORIDE;thiophenyl chloride;Phenylsulfinyl chloride;Chloro phenyl sulfoxide;Benzenesulfinic chloride
CAS:4972-29-6
MF:C6H5ClOS
MW:160.62
EINECS:
Product Categories:
Mol File:4972-29-6.mol
BENZENESULFINYL CHLORIDE Structure
BENZENESULFINYL CHLORIDE Chemical Properties
Melting point 38°C
Boiling point 117.5°C (estimate)
density 1.347
refractive index 1.3470
form solid
color Plates
Safety Information
MSDS Information
BENZENESULFINYL CHLORIDE Usage And Synthesis
Synthesis Reference(s)Tetrahedron Letters, 33, p. 3973, 1992 DOI: 10.1016/0040-4039(92)88076-H
Safety ProfileMay explode if stored in a sealedcontainer. When heated to decomposition it emits toxicfumes of SOx and Cl-.
SynthesisA mixture of 30.4 g (0.2 mol) of phenyl thioacetate and 20.4 g (0.2 mol) of acetic anhydride is chlorinated at -10 to 0℃. The color changes to yellow, then red, and then back to yellow. The reaction mixture is heated to 80℃ under reduced pressure (3.5 kPa), until the residue begins to boil, after which it is cooled; yield: 31.5–31.8 g (98.1– 99.1%).
BENZENESULFINYL CHLORIDE Preparation Products And Raw materials
Preparation ProductsN-TERT-BUTYLBENZENESULFENAMIDE-->METHYL BENZENESULFINATE-->PROPARGYL BENZENESULFONATE
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