Company Name: |
Bide Pharmatech Ltd.
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Tel: |
400-1647117 15221909166 |
Email: |
product02@bidepharm.com |
Products Intro: |
Product Name:Benzenesulfinic chloride CAS:4972-29-6 Purity:95% Package:250mg;1g;5g Remarks:BD00733391
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| BENZENESULFINYL CHLORIDE Basic information |
Product Name: | BENZENESULFINYL CHLORIDE | Synonyms: | BENZENESULFINYL CHLORIDE;thiophenyl chloride;Phenylsulfinyl chloride;Chloro phenyl sulfoxide;Benzenesulfinic chloride | CAS: | 4972-29-6 | MF: | C6H5ClOS | MW: | 160.62 | EINECS: | | Product Categories: | | Mol File: | 4972-29-6.mol | |
| BENZENESULFINYL CHLORIDE Chemical Properties |
Melting point | 38°C | Boiling point | 117.5°C (estimate) | density | 1.347 | refractive index | 1.3470 | form | solid | color | Plates |
| BENZENESULFINYL CHLORIDE Usage And Synthesis |
Synthesis Reference(s) | Tetrahedron Letters, 33, p. 3973, 1992 DOI: 10.1016/0040-4039(92)88076-H | Safety Profile | May explode if stored in a sealedcontainer. When heated to decomposition it emits toxicfumes of SOx and Cl-. | Synthesis | A mixture of 30.4 g (0.2 mol) of phenyl thioacetate and 20.4 g (0.2 mol) of acetic anhydride is chlorinated at -10 to 0℃. The color changes to yellow, then red, and then back to yellow. The reaction mixture is heated to 80℃ under reduced pressure (3.5 kPa), until the residue begins to boil, after which it is cooled; yield: 31.5–31.8 g (98.1– 99.1%). |
| BENZENESULFINYL CHLORIDE Preparation Products And Raw materials |
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