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ChemicalBook CAS DataBase List 1,2-Diiodobenzene

1,2-Diiodobenzene synthesis

13synthesis methods
-

Yield:-

Reaction Conditions:

with iodine;oxygen at 280; under 760.051 Torr; for 24 - 400 h;Product distribution / selectivity;

Steps:

1; 5; 6
In the system shown in FIG. 1, benzene (26.4 g/hr) and iodine (42.9 g/hr) were fed into a reactor without adding monoiodobenzene, and were subjected to a continuous iodination process under conditions of a reaction temperature of 280 °C and atmospheric pressure. 24 hours after the reaction conditions were reached, sampling and analysis were performed. The experimental conditions and results are shown in Table 1 below.

References:

SK CHEMICALS CO., LTD. WO2009/54555, 2009, A1 Location in patent:Page/Page column 9-12

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