ChemicalBook CAS DataBase List 1-ACENAPHTHENOL

1-ACENAPHTHENOL synthesis

13synthesis methods

Product Name:1-ACENAPHTHENOL
CAS Number:6306-07-6
Molecular formula:C12H10O
Molecular Weight:170.21

2235-15-6 Synthesis

2235-15-6
117 suppliers
$100.00/1 g

6306-07-6
88 suppliers
$26.50/1g

Yield: 94.2%

Reaction Conditions:

with hydrogen in methanol at 100; under 30003 Torr;Autoclave;Temperature;

Steps:

2.1
1) In a 1000 ml autoclave, 700 ml of methanol was added as a solvent,Followed by the addition of 168 gl-acenaphthene, 13 g hydrogenation catalyst nickel catalyst AMG-1200; added to complete, sealed reactor,First use the nitrogen to replace the kettle air twice, through the H2 to the pressure4.OMPa, open the stirring, heating to 100 ° C to react, the reaction to no hydrogen,1-naphthenaphthene was removed and the reaction was stopped,Followed by column purification of 1 - hydroxy acenaphthalene pure product 160.14g, the yield was 94.2%

References:

Wang Jiju CN106397116, 2017, A Location in patent:Paragraph 0012