1-Boc-3-pyrrolidinecarbaldehyde synthesis
- Product Name:1-Boc-3-pyrrolidinecarbaldehyde
- CAS Number:59379-02-1
- Molecular formula:C10H17NO3
- Molecular Weight:199.25
114214-69-6
219 suppliers
$6.00/250mg
59379-02-1
195 suppliers
$12.00/250mg
Yield: 93%
Reaction Conditions:
with manganese(IV) oxide in dimethyl sulfoxide at 20; for 24 h;Solvent;Reagent/catalyst;
Steps:
3.4 Example 3:
1 kg of N-Boc-pyrrolidine-3-methanol was dissolved in 5 liters of DMSO,Room temperature by adding manganese dioxide 2.14kg,Room temperature reaction for about 24 hours,Reaction is completed,filter,Spin dry solvent,N-Boc-pyrrolidine-3-carbaldehyde (920 g) was distilled off under reduced pressure,Yield 93%.
References:
Wuhan Hengda of Biomedical Co., Ltd.;Zhou, Yebing;Lu, Dongan;Liu, Jie;Zhang, Shengbo CN106588738, 2017, A Location in patent:Paragraph 0036; 0041; 0042; 0046; 0047; 0048
569667-93-2
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$247.50/1g
59379-02-1
195 suppliers
$12.00/250mg
201230-82-2
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73286-71-2
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59378-82-4
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59379-02-1
195 suppliers
$12.00/250mg
201230-82-2
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73286-70-1
291 suppliers
$6.00/5g
59378-82-4
10 suppliers
inquiry
59379-02-1
195 suppliers
$12.00/250mg
201230-82-2
1 suppliers
inquiry
73286-70-1
291 suppliers
$6.00/5g
59379-02-1
195 suppliers
$12.00/250mg