ChemicalBook CAS DataBase List 4-(ethylaMino)-2-(Methylthio)pyriMidine-5-carbaldehyde

4-(ethylaMino)-2-(Methylthio)pyriMidine-5-carbaldehyde synthesis

4synthesis methods

Product Name:4-(ethylaMino)-2-(Methylthio)pyriMidine-5-carbaldehyde
CAS Number:185040-35-1
Molecular formula:C8H11N3OS
Molecular Weight:197.26

5909-24-0 Synthesis

Ethyl 4-chloro-2-methylthio-5-pyrimidinecarboxylate

5909-24-0
402 suppliers
$6.00/5g

4-(ethylaMino)-2-(Methylthio)pyriMidine-5-carbaldehyde

185040-35-1
34 suppliers
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 90 percent / Et₃N / tetrahydrofuran; H₂O / 0.5 h / 20 °C
2: 92 percent / LiAlH₄ / tetrahydrofuran / 0.17 h / 20 °C
3: 97 percent / MnO₂ / CHCl₃ / 6.5 h / 20 °C

References:

Barvian;Boschelli;Cossrow;Dobrusin;Fattaey;Fritsch;Fry;Harvey;Keller;Garrett;La;Leopold;McNamara;Quin;Trumpp-Kallmeyer;Toogood;Wu;Zhang [Journal of Medicinal Chemistry,2000,vol. 43,# 24,p. 4606 - 4616]

185040-34-0 Synthesis

(4-(ethylaMino)-2-(Methylthio)pyriMidin-5-yl)Methanol

185040-34-0
16 suppliers
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185040-35-1
34 suppliers
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References

ETHYL 4-(ETHYLAMINO)-2-(METHYLTHIO)PYRIMIDINE-5-CARBOXYLATE

185040-33-9
20 suppliers
$100.00/250mg

185040-35-1
34 suppliers
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References

5909-24-0 Synthesis

5909-24-0
402 suppliers
$6.00/5g

75-04-7
370 suppliers
$10.00/20mg

185040-35-1
34 suppliers
inquiry

References