2,3-DIHYDRO-1,4-BENZODIOXIN-6-YLMETHYLAMINE synthesis
- Product Name:2,3-DIHYDRO-1,4-BENZODIOXIN-6-YLMETHYLAMINE
- CAS Number:17413-10-4
- Molecular formula:C9H11NO2
- Molecular Weight:165.19
![(E)-2,3-dihydrobenzo[b][1,4]dioxine-6-carbaldehyde oxiMe](/CAS/GIF/31127-39-6.gif)
31127-39-6
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$14.00/100mg
17413-10-4
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$45.00/50mg
Yield:-
Reaction Conditions:
with hydrogen;palladium(II) hydroxide in ethanol at 30 - 60; for 6 h;
Steps:
234 Example 234: Preparation of 1,4-benzodioxan-7-methylamine (Intermediate XXVI).
177 mg of the intermediate XXV was dissolved in ethanol, a catalytic amount of palladium hydroxide was added, the air was replaced and hydrogen was introduced, and the reaction was carried out at 30-60° C. for 6 hours. After the reaction was completed, ethanol was distilled off under reduced pressure, and water was added to the residue. Ester extraction, without purification, gives the intermediate 1,4-benzodioxane-7-methylamine directly for the next reaction
References:
East China University of Science and Technology;Chinese Academy Of Sciences Shanghai Pharmaceutical Institute;Li Jian;Lan Lefu;Ni Shuaishuai;Chen Feifei;Wei Hanwen;Li Baoli;Liu Yifu;Mao Fei;Zhu Jin CN108117534, 2018, A Location in patent:Paragraph 1180; 1181; 1182
29668-44-8
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$6.00/1g
17413-10-4
98 suppliers
$45.00/50mg
124362-47-6
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17413-10-4
98 suppliers
$45.00/50mg