ChemicalBook CAS DataBase List 2,4-Dinitrodiphenylamine

2,4-Dinitrodiphenylamine synthesis

15synthesis methods

Product Name:2,4-Dinitrodiphenylamine
CAS Number:961-68-2
Molecular formula:C12H9N3O4
Molecular Weight:259.22

Aniline and 1-Chloro-2,4-dinitrobenzene?condensation

62-53-3 Synthesis

62-53-3
631 suppliers
$10.00/1g

97-00-7
12 suppliers
$17.67/10gm:

961-68-2
100 suppliers
$39.00/25g

Yield: 95%

Reaction Conditions:

in neat (no solvent) at 30; for 0.166667 h;Green chemistry;Reagent/catalyst;

Steps:

2.3 General Procedure for DES Catalyzed N-Arylationof Amines with Aryl Halides
General procedure: To a solution of amine (1.2 mmol) dissolved in 20% DES,aryl halide (1 mmol) was added at room temperature andstirred for appropriate time. The progress of the reactionwas monitored by TLC. After completion of the reactioncold water was added to the reaction mixture. The precipitatedsolid was filtered off, and recrystallized using ethanol.

References:

Pant, Preeti Lalit;Shankarling, Ganapati Subray [Catalysis Letters,2017,vol. 147,# 6,p. 1371 - 1378]

70-34-8 Synthesis