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ChemicalBook CAS DataBase List 2-FLUORO-5-(TRIFLUOROMETHYL)PHENYLBORONIC ACID

2-FLUORO-5-(TRIFLUOROMETHYL)PHENYLBORONIC ACID synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: Bis<2-(N,N-dimethylamino)aethyl>aether / hexane / 1.5 h / -15 - -5 °C / Inert atmosphere
2.1: Bis<2-(N,N-dimethylamino)aethyl>aether / hexane / -15 - 20 °C / Inert atmosphere
2.2: 20 °C

References:

Nippon Soda Co., Ltd. US2011/224457, 2011, A1

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