2-Naphthoyl chloride synthesis
- Product Name:2-Naphthoyl chloride
- CAS Number:2243-83-6
- Molecular formula:C11H7ClO
- Molecular Weight:190.63
93-09-4
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2243-83-6
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Yield:2243-83-6 100%
Reaction Conditions:
with thionyl chloride for 4 h;Heating / reflux;
Steps:
1
A 100 mL round bottom flask was charged with 2-naphthoic acid (2 g, 11.6 mmol) and SOCl2 (15 mL). The solution was refluxed for 4 hours and then concentrated to yield a yellow solid which was used without further purification (2.21 g, 100% yield); 1H NMR (CDCl3) δ 8.76 (s, 1H, ArH), 8.04 (2H, ArH), 7.93 (d, 2H, ArH, J=8.9 Hz), 7.66 (m, 2H, ArH).
References:
Prendergast, George C.;Malachowski, William P.;Muller, Alexander J.;DuHadaway, James B. US2007/105907, 2007, A1 Location in patent:Page/Page column 10
93-08-3
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2243-83-6
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115298-62-9
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2243-83-6
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3857-83-8
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141-75-3
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2243-83-6
209 suppliers
$6.00/5g
