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ChemicalBook CAS DataBase List 3,7,3',4'-TETRAMETHYLGOSSYPETIN

3,7,3',4'-TETRAMETHYLGOSSYPETIN synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 86 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.5 h / 0 - 20 °C
2: 96 percent / K2CO3 / acetone / 1 h / Heating
3: 99 percent / BBr3 / CH2Cl2 / 0.5 h / 0 °C
4: 89 percent / dimethyl dioxirane / acetone; CH2Cl2 / 0.83 h / 0 - 20 °C

References:

Chu, Han-Wei;Wu, Huan-Ting;Lee, Yean-Jang [Tetrahedron,2004,vol. 60,# 11,p. 2647 - 2655]

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