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ChemicalBook CAS DataBase List 3-BROMOTHIOPHENE-2-CARBONITRILE

3-BROMOTHIOPHENE-2-CARBONITRILE synthesis

4synthesis methods
-

Yield: 100 %Spectr.

Reaction Conditions:

with 1-methyl-3-(4-sulfonylbutyl)-1H-imidazol-3-ium trifluoromethanesulfonate;trimethylsilylazide;3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate at 20 - 50; for 3 h;Sonication;Schmidt Reaction;

References:

Nandi, Ganesh C.;Laali, Kenneth K. [Tetrahedron Letters,2013,vol. 54,# 17,p. 2177 - 2179]

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