ChemicalBook CAS DataBase List 3-NITROPHENYL ISOTHIOCYANATE

3-NITROPHENYL ISOTHIOCYANATE synthesis

12synthesis methods

Product Name:3-NITROPHENYL ISOTHIOCYANATE
CAS Number:3529-82-6
Molecular formula:C7H4N2O2S
Molecular Weight:180.18

280-57-9 Synthesis

280-57-9
556 suppliers
$5.00/5g

75-15-0
233 suppliers
$40.00/100 g

99-09-2 Synthesis

99-09-2
10 suppliers
$14.00/1g

3529-82-6
89 suppliers
$28.00/1g

Yield: 64.7%

Reaction Conditions:

in toluene at 20; for 10 h;

Steps:

29.1 Example 29:
Example 29:
1) 15. 0mmol3- nitroaniline, 4. 62mmol triethylenediamine was added to the eggplant-shaped flask 50mL, 10. OmL toluene was added, stirring was started at room temperature while a solution of 0. 90mL CS2, followed by stirring at room temperature 10h, filtration, filtration and air dry the resulting solid to give a yellow powder 3-nitrophenyl dithiocarbamate three ethylene diammonium salt (3. 15g, 64. 7%), see formula Scheme 60).

References:

Xi'an Jiaotong University;Meng, Ge;Tong, Jing;Shi, Jianhua;Tian, Chao;Bo, Yusi;Yang, Lingfei;Naibi, Nusire CN103992265, 2016, B Location in patent:Paragraph 0212; 0213; 0214