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ChemicalBook CAS DataBase List 4,4-DIMETHYLCYCLOHEXEN-1-YLBORONIC ACID

4,4-DIMETHYLCYCLOHEXEN-1-YLBORONIC ACID synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: methanol / 2 h / 70 °C / Reflux
2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / hexane / 3 h / -78 - 25 °C
2.2: -78 °C
3.1: water; sodium periodate; ammonium acetate / acetone

References:

Bi, Hong-Yan;Li, Cheng-Jing;Liang, Cui;Mo, Dong-Liang;Wei, Cui [Green Chemistry,2020,vol. 22,# 17,p. 5815 - 5821]

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