4-(CHLOROSULFONYL)PHENYL ISOCYANATE synthesis
1synthesis methods
- Product Name:4-(CHLOROSULFONYL)PHENYL ISOCYANATE
- CAS Number:6752-38-1
- Molecular formula:C7H4ClNO3S
- Molecular Weight:217.63
Yield:6752-38-1 70%
Reaction Conditions:
in N,N-dimethyl-formamide;1,2-dichloro-benzene at 165;Condensation;chlorination;
References:
Chung, John Y. L.;Ho, Guo-Jie;Chartrain, Michel;Roberge, Chris;Zhao, Dalian;Leazer, John;Farr, Roger;Robbins, Micheal;Emerson, Kateeta;Mathre, David J.;McNamara, James M.;Hughes, David L.;Grabowski, Edward J. J.;Reider, Paul J. [Tetrahedron Letters,1999,vol. 40,# 37,p. 6739 - 6743]