4-Methylmorpholine N-oxide synthesis
- Product Name:4-Methylmorpholine N-oxide
- CAS Number:7529-22-8
- Molecular formula:C5H11NO2
- Molecular Weight:117.15
109-02-4
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7529-22-8
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Yield:7529-22-8 100%
Reaction Conditions:
with carbon dioxide;phosphoric acid;dihydrogen peroxide under 7500.75 Torr; for 0.133333 h;Autoclave;Reagent/catalyst;Pressure;Time;
Steps:
EXAMPLES
Execution of the Reaction in the Microreactor
The microreaction system used by us is based on WO 2010/055034 and was produced from the material [A] according to the table.
The microreactor tests for the synthesis of N-methylmorpholine N-oxide (NMMNO) from 4-N-methylmorpholine (NMM) and hydrogen peroxide (H2O2) were carried out in different fittings in the microreactor.
The characteristic data of the used reactor (1) are as follows:
volume: variable, up to 26 mL
References:
US2019/300493,2019,A1 Location in patent:Paragraph 0079
109-02-4
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76847-41-1
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7529-22-8
378 suppliers
$5.00/1g