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ChemicalBook CAS DataBase List 5-(3-METHOXY-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE

5-(3-METHOXY-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE synthesis

6synthesis methods
-

Yield:247109-15-5 84%

Reaction Conditions:

Stage #1: thiosemicarbazide;3-Methoxybenzoic acidwith trichlorophosphate at 75; for 1 h;
Stage #2: with lithium hydroxide monohydrate at 20; for 4 h;Reflux;

References:

Alegaon, Shankar G.;Alagawadi, Kallanagouda R. [Medicinal Chemistry Research,2012,vol. 21,# 6,p. 816 - 824] Location in patent:experimental part

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