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ChemicalBook CAS DataBase List 5-Mercapto-1H-tetrazole-1-acetic acid

5-Mercapto-1H-tetrazole-1-acetic acid synthesis

1synthesis methods
-

Yield:-

Reaction Conditions:

with sodium hydroxide

Steps:

R.22.3 REFERENCE EXAMPLE 22

(3) Using a solution of sodium hydroxide, 1-N,N-dimethylcarbamoylmethyl-1H-tetrazole-5-thiol is hydrolyzed to obtain 1-carboxymethyl-1H-tetrazole-5-thiol. melting point: 156°-160° C. (decomp.) IR (KBr, cm-1): 1713 NMR (60 MHz, in d6 -DMSO) δ: 5.03 (s, CH2 CO), 12.09 (br. s, NH & --COOH)

References:

US4278671,1981,A

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