6-Aminoquinoxaline synthesis
- Product Name:6-Aminoquinoxaline
- CAS Number:6298-37-9
- Molecular formula:C8H7N3
- Molecular Weight:145.16
615-47-4
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$8.00/1g
6298-37-9
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$14.14/1gm:
Yield:6298-37-9 87%
Reaction Conditions:
in water;sodium carbonate
Steps:
1 6-Aminoquinoxaline
6-Aminoquinoxaline Glyoxal sodium bisulfite adduct (Aldrich, 14.3g, 50 mmol) was added in small portions to a solution of 1,2,4-triaminobenzene dihydrochloride (9.8 g, 50 mmol) in 200 ml of 10% by weight sodium carbonate in water. The reaction mixture was heated to 100° C. for two hours and then cooled to 0° C. The crystals formed were filtered off and dried in vacuo to give a crude yield of 7.06 g (a yield of 97%) of brown crystals. Recrystallization from benzene gave 6.32 g (a yield of 87%) yellow crystals, m.p. 157-8° C. Using various analytical procedures, these yellow crystals were determined to be 6-aminoquinoxaline.
References:
Allergan US6323204, 2001, B1
6639-87-8
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$15.00/100mg
6298-37-9
268 suppliers
$14.14/1gm:
5448-43-1
70 suppliers
$15.00/1g
6298-37-9
268 suppliers
$14.14/1gm:
50998-17-9
179 suppliers
$6.00/250mg
6298-37-9
268 suppliers
$14.14/1gm:
50998-18-0
51 suppliers
$69.00/100mg
6298-37-9
268 suppliers
$14.14/1gm: