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ChemicalBook CAS DataBase List 6-chloro-5-Methyl-2,3-dihydroinden-1-one

6-chloro-5-Methyl-2,3-dihydroinden-1-one synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 75 percent / H2 / Pd/C / ethanol / 1 h / 20 °C / 1520 Torr
2.1: aq. NaNO2; aq. HCl / 0 °C
2.2: 100 percent / CuCl; aq. HCl / 24 h / 0 - 20 °C

References:

Murineddu, Gabriele;Lazzari, Paolo;Ruiu, Stefania;Sanna, Angela;Loriga, Giovanni;Manca, Ilaria;Falzoi, Matteo;Dessì, Christian;Curzu, Maria M.;Chelucci, Giorgio;Pani, Luca;Pinna, Gérard A. [Journal of Medicinal Chemistry,2006,vol. 49,# 25,p. 7502 - 7512]

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