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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 6-Nitrophthalide

6-Nitrophthalide synthesis

11synthesis methods
6-Nitrophthalide is synthesized from 2-nitrobenzaldehyde via a two-step process, and then reacted with methyl iodide.
85-44-9 Synthesis
Phthalic anhydride

85-44-9
749 suppliers
$9.00/5g

6-Nitrophthalide

610-93-5
138 suppliers
$6.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate / tetrahydrofuran / 12 h / 0 - 20 °C
1.2: 12 h / 20 °C / pH 1
2.1: nitric acid; sulfuric acid / 12 h / 0 - 20 °C

References:

Santoso, Kristiana T.;Cheung, Chen-Yi;Hards, Kiel;Cook, Gregory M.;Stocker, Bridget L.;Timmer, Mattie S. M. [Chemistry - An Asian Journal,2019,vol. 14,# 8,p. 1278 - 1285]

87-41-2 Synthesis
Phthalide

87-41-2
456 suppliers
$6.00/10g

6-Nitrophthalide

610-93-5
138 suppliers
$6.00/1g

References
5466-84-2 Synthesis
4-Nitrophthalic anhydride

5466-84-2
233 suppliers
$11.00/1g

6-Nitrophthalide

610-93-5
138 suppliers
$6.00/1g

References
2-Methyl-5-nitrobenzoic acid

1975-52-6
276 suppliers
$12.00/1 g

6-Nitrophthalide

610-93-5
138 suppliers
$6.00/1g

References
5466-84-2 Synthesis
4-Nitrophthalic anhydride

5466-84-2
233 suppliers
$11.00/1g

6-Nitrophthalide

610-93-5
138 suppliers
$6.00/1g

1(3H)-Isobenzofuranone, 5-nitro-

67081-02-1
6 suppliers
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(4-nitro-1,2-phenylene)diMethanol

22162-19-2
9 suppliers
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References

6-Nitrophthalide Related Search:

3-Nitrobenzaldehyde 4-Nitrophthalic anhydride Phthalide