6-Propyl-2-naphthol synthesis
- Product Name:6-Propyl-2-naphthol
- CAS Number:2776-56-9
- Molecular formula:C13H14O
- Molecular Weight:186.25
94134-18-6
42 suppliers
$194.00/250mg
2776-56-9
68 suppliers
$40.00/10mg
Yield:2776-56-9 55.1 g
Reaction Conditions:
with boron tribromide in dichloromethane at 0 - 20; for 6 h;Inert atmosphere;
Steps:
2.2-2
under a nitrogen atmosphere, 2-methoxy-6-propyl-naphthalene (74.2g) in dichloromethane (550mL) in 1mol / L boron tribromide dichloromethane solution (550mL) was added dropwise at 0°C , in 2 hours, and the mixture was stirred for 4 hours at room temperature. The reaction mixture was added to ice water, after separation of the aqueous layer was extracted twice with dichloromethane, The combined organic layers were washed with saturated brine, dried over anhydrous sodium sulfate.. The solvent was evaporated under reduced pressure to give 6-propyl-naphthalene-2-ol(55.1g).
References:
DIC CORPORATION;HAYASHI, TAKUO;AOKI, YOSHIO;OHASHI, YUJI;TANIGUCHI, SHIROU;TOJO, KENTA JP2016/8207, 2016, A Location in patent:Paragraph 0211; 0212
15231-91-1
392 suppliers
$7.00/5g
107-08-4
247 suppliers
$14.00/5g
2776-56-9
68 suppliers
$40.00/10mg
5111-65-9
329 suppliers
$6.00/5g
2776-56-9
68 suppliers
$40.00/10mg
94134-18-6
42 suppliers
$194.00/250mg
628-13-7
410 suppliers
$9.00/25g
2776-56-9
68 suppliers
$40.00/10mg