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ChemicalBook CAS DataBase List cis-3-Hexenyl Acetate

cis-3-Hexenyl Acetate synthesis

10synthesis methods
By acetylation of the corresponding alcohol
-

Yield:3681-71-8 70%

Reaction Conditions:

with Candida antarctica lipase B immobilized on a macroporous acrylic resin at 40; for 19 h;Green chemistry;Enzymatic reaction;Temperature;

Steps:

General experiment for the optimised acetylation of alcohols, according to Scheme 2:
General procedure: Lipozyme 435 (2percent wt) was added to a solution of an alcohol (1 equiv) in EGDA (2 equiv).The reaction mixture was incubated in an orbital shaker (40 °C, 150 rpm) and the reaction progress wasmonitored by GC-FID (see Table 1).

References:

Puchl'Ová, Eva;Szolcsányi, Peter [Molecules,2020,vol. 25,# 14] Location in patent:supporting information

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