ChemicalBook CAS DataBase List DIISOBUTYLALUMINUM CHLORIDE

DIISOBUTYLALUMINUM CHLORIDE synthesis

8synthesis methods

Product Name:DIISOBUTYLALUMINUM CHLORIDE
CAS Number:1779-25-5
Molecular formula:C8H18AlCl
Molecular Weight:176.66

7446-70-0 Synthesis

7446-70-0
683 suppliers
$15.00/25g

100-99-2 Synthesis

100-99-2
97 suppliers
$81.09/100ml

563-43-9 Synthesis

563-43-9
76 suppliers
$12.19/10ml

1779-25-5
72 suppliers
$45.00/10g

Yield:-

Reaction Conditions:

in diethyl ether;tolueneall manipulations under dry, O2 free N2 atm.; AlCl3 dissolved in Et2O, soln. of iso-Bu3Al in toluene added at -78°C, allowed to warm to room temp., stirred and refluxed for for 3, stirred at room temp. for 48 h h;

References:

Schumann, Herbert;Dechert, Sebastian;Hummert, Markus;Lange, Katharina C. H.;Schutte, Stefan;Wassermann, Birgit C.;Koehler, Katrin;Eichhorn, Jens [Zeitschrift fur Anorganische und Allgemeine Chemie,2004,vol. 630,# 8-9,p. 1196 - 1204]