Ethyl 3-ethoxypropionate synthesis
- Product Name:Ethyl 3-ethoxypropionate
- CAS Number:763-69-9
- Molecular formula:C7H14O3
- Molecular Weight:146.18
64-17-5
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140-88-5
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763-69-9
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Yield:763-69-9 98%
Reaction Conditions:
with quaternary ammonium salt anion exchange resin in lithium hydroxide monohydrate at 30; for 4 h;Inert atmosphere;Temperature;
Steps:
1-19 Specific Example 19:
Adding absolute ethanol and ethyl acrylate to a 2-liter four-necked flask and before Example 19A total of 1500 grams of the fraction of anhydrous ethanol: ethyl acrylate, controlled temperature of 30 degrees ± 2 degrees, added to the catalyst of Example 18, stirring, rotating at a speed of not more than 120 rpm, the catalyst suspension dispersion is uniform, after 4 hours of reaction, Stirring was stopped, the catalyst was filtered off, and the ethyl acrylate content in the filtrate was determined to be 0.5%.The filtrate is added to the column of the rectification column, heated, and slowly rectified between 74-165 degrees to remove the ethanol and ethyl acrylate and a small amount of the forward fraction of ethyl 3-ethoxypropionate.99% of the product was collected with a yield of 98%.The catalyst is regenerated by recycling to the ethyl acrylate reaction until the end point content is above 1%.
References:
CN108569965,2018,A Location in patent:Paragraph 0042-0050
917-58-8
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140-88-5
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$12.00/100ml
763-69-9
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$14.00/25mL
141-52-6
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140-88-5
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$12.00/100ml
763-69-9
311 suppliers
$14.00/25mL
64-17-5
699 suppliers
$10.00/50g
3586-58-1
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763-69-9
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$14.00/25mL
462-95-3
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763-69-9
311 suppliers
$14.00/25mL