ChemicalBook CAS DataBase List N-(4-METHOXYBENZYLIDENE)ANILINE

N-(4-METHOXYBENZYLIDENE)ANILINE synthesis

15synthesis methods

Product Name:N-(4-METHOXYBENZYLIDENE)ANILINE
CAS Number:836-41-9
Molecular formula:C14H13NO
Molecular Weight:211.26

62-53-3 Synthesis

62-53-3
631 suppliers
$10.00/1g

768-60-5
217 suppliers
$6.00/1g

836-41-9
68 suppliers
$29.00/5g

Yield: 92%

Reaction Conditions:

with C₂₆H₂₁BiClN in chloroform at 100; for 10 h;Reagent/catalyst;

Steps:

35 Catalytic activity test:
Add 0.5 mmol of phenylacetylene to the 10 mL reaction tube (R1, R2, R4, R5 are hydrogen, R3 is methoxy), 0.5 mmol aniline(R6, R7, R8, R9, R10 are hydrogen),0.015 mmol of the novel organic rhodium complex catalyst obtained in Example 35,Then add 2ml of chloroform,The reaction tube was placed in a heater at 100 ° C for 10 h.After the reaction is completed,The target compound is isolated by column chromatography.The yield was 92%.

References:

Hunan University;Qiu Renhua;Zhang Dejiang CN109206453, 2019, A Location in patent:Paragraph 0169; 0170; 0172; 0173; 0177; 0181

3526-43-0 Synthesis