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ChemicalBook CAS DataBase List N-OLEOYLSARCOSINE

N-OLEOYLSARCOSINE synthesis

4synthesis methods
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Yield:110-25-8 84%

Reaction Conditions:

with bis(perfluorohexylsulfonic acid) zirconocene in lithium hydroxide monohydrate;propan-2-one at 100; for 24 h;

Steps:

30 Example 30

A round bottom flask (100 mL) was charged with catalyst bis(perfluorohexylsulfonic acid) zirconocene (0.0888 g, 0.1 mmol), oleic acid (2.8245 g, 10 mmol), sarcosine (0.8909 g, 10 mmol) and acetone/water The mixed solvent (30 mL) was reacted at 100° C. for 24 h, the reaction was stopped, the solvent was removed, and ethanol/petroleum ether mixed solvent was added to the solid compound, and the mixture was crystallized for 24 h to obtain oleoyl sarcosine with a yield of 84%.

References:

CN114031516,2022,A Location in patent:Paragraph 0097-0098

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