Olivetol synthesis

12synthesis methods

Product Name:Olivetol
CAS Number:500-66-3
Molecular formula:C11H16O2
Molecular Weight:180.24

Olivetol has a variety of biological activities, and has killing effect on fungi and bacteria of various pathogens. It can be synthesized by nitration, amination and aminohydroxylation after the reaction of benzene and n-valeryl chloride.
synthesis of Olivetol

22976-40-5
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500-66-3
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Yield:500-66-3 97.1%

Reaction Conditions:

with pyridine hydrochloride at 150; for 2 h;Inert atmosphere;Reagent/catalyst;Temperature;

Steps:

1.4; 3.4

(4). Heat pyridine hydrochloride (1mol, 116g) at 150 to melt into liquid, under the protection of nitrogen,Add 3,5-dimethoxypentylbenzene (1mol, 208g), keep at 150 and react for 2h, then cool the reaction liquid,Then pour into 500mL cold water, extract twice with ether, combine the organic phases and wash with water, dry and concentrate with anhydrous magnesium sulfate to obtain a pale yellow viscous oily liquid 3,5-dihydroxypentabenzene (175g, 97.1%)

References:

CN112939738,2021,A Location in patent:Paragraph 0042-0043; 0047; 0054-0055; 0059

27871-89-2 Synthesis

methyl 6-n-pentyl-2-hydroxy-4-oxo-cyclohex-2-ene-1-carboxylate

27871-89-2
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500-66-3
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58016-28-7 Synthesis

58016-28-7
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500-66-3
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References

1,3-Benzenedicarboxylic acid, 2,4-dihydroxy-6-pentyl-, 1,3-dimethyl ester

53103-15-4
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500-66-3
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1132-21-4 Synthesis

1132-21-4
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500-66-3
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References

Olivetol Related Search:

4-Hydroxybenzaldehyde Methylparaben 4-Methoxyphenol 4-Chlororesorcinol 4-Hydroxybenzoic acid 2-Nitroresorcinol Triclosan Resorcinol Acetic acid Glycerol