ChemicalBook CAS DataBase List Repaglinide Impurity 16

Repaglinide Impurity 16 synthesis

7synthesis methods

Product Name:Repaglinide Impurity 16
CAS Number:219921-93-4
Molecular formula:C16H26N2
Molecular Weight:246.4

Benzenemethanamine, α-(2-methyl-2-propen-1-yl)-2-(1-piperidinyl)-N-[[2-(1-piperidinyl)phenyl]methylene]-, [N(E)]-

1026508-90-6
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219921-93-4
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: HCl / 0.5 h / 0 °C
2: Ambient temperature
3: Ti(OiPr)4 / tetrahydrofuran; toluene / 60 h / 100 °C
4: H₂, aq. HCl / 10 percent Pd/C / 5 h / 50 °C / 3750.3 Torr

References:

Grell, Wolfgang;Hurnaus, Rudolf [Journal of Medicinal Chemistry,1998,vol. 41,# 26,p. 5219 - 5246]

Benzenemethanamine, α-(2-methylpropyl)-N-[(1S)-1-phenylethyl]-2-(1-piperidinyl)-, (αS)-

147770-01-2
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219921-93-4
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147769-93-5 Synthesis

(S)-3-Methyl-1-(2-piperidin-1-ylphenyl)butylamine

147769-93-5
194 suppliers
$34.00/250mg

References

Benzenemethanamine, α-(2-methylpropyl)-N-[(1R)-1-phenylethyl]-2-(1-piperidinyl)-, (αS)-

219922-07-3
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219921-93-4
6 suppliers
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147769-93-5 Synthesis

147769-93-5
194 suppliers
$34.00/250mg

References

Benzenemethanamine, α-(2-methylpropyl)-N-[(1R)-1-phenylethyl]-2-(1-piperidinyl)-, (αR)-

219921-97-8
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219921-93-4
6 suppliers
inquiry

147769-93-5 Synthesis

147769-93-5
194 suppliers
$34.00/250mg

References

147769-96-8
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219921-93-4
6 suppliers
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References

Repaglinide Impurity 16 Related Search:

4-ETHYL-2-FLUORO-1,1'-BIPHENYL 3-Ethoxy-4-ethoxycarbonyl phenylacetic acid (4-Carboxy-3-ethoxy)phenyl Acetic Acid (Repaglinide Impurity) (+)-2-Ethoxy-4-(N-3-Methyl-1(S)-(2-(1-Piperidinyl)Phenyl)-Butyl)Carbamoylmethyl)