(S)-2-AMINO-2-CYCLOHEXYL-ETHANOL synthesis
- Product Name:(S)-2-AMINO-2-CYCLOHEXYL-ETHANOL
- CAS Number:845714-30-9
- Molecular formula:C8H17NO
- Molecular Weight:143.23
14328-51-9
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845714-30-9
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Yield: 85%
Reaction Conditions:
with lithium aluminium tetrahydride in tetrahydrofuran for 6 h;Cooling with ice;Reflux;
Steps:
1 Synthesis of Ligand L1 of Example 1
Under ice bath, in lOOmL LiAlH4 (160mmol)Slowly add 1 (80 mmol) of 100 mL THF solution to the THF solution.After the addition is completed, the temperature is naturally raised to room temperature, and then the heating is stopped after heating for 6 hours.The reaction was quenched with water under ice-bath, extracted with DCM, dried over Na 2After removing the solvent, directly put it into the next step
References:
Chinese Academy Of Sciences Shanghai Organic Chemistry Institute;Tang Yong;Hu Jianglin;Xie Zuowei;Kang Qikai;Liu Qiongjie;Cheng Yujing CN104926747, 2018, B Location in patent:Paragraph 0252-0254
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1000210-73-0
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845714-30-9
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5664-29-9
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845714-30-9
76 suppliers
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1000210-73-0
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845714-30-9
76 suppliers
$23.00/250mg
1000210-73-0
0 suppliers
inquiry
845714-30-9
76 suppliers
$23.00/250mg