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ChemicalBook CAS DataBase List TETRAETHYLLEAD

TETRAETHYLLEAD synthesis

11synthesis methods
Lead tetraethyl is prepared by heating ethyl chloride in the presence of a catalyst in an autoclave at 40 to 60°C with an alloy of lead and sodium:
Pb + 4Na + 4C2H5Cl → Pb(C2H5)4 + 4NaCl
Also, it can be prepared by the reaction of lead with ethylene and hydrogen in the presence of Ziegler catalyst, triethylaluminum:
Pb + 4C2H4 + 2H2 → Pb(C2H5)4
-

Yield:-

Reaction Conditions:

in diethyl etherElectrolysis; with Pb anode;

References:

[Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Bi: Org.Verb., 1.3.3.1.1, page 46 - 55]

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