ChemicalBook--->CAS DataBase List--->32014-70-3

32014-70-3

32014-70-3 Structure

32014-70-3 Structure
IdentificationMore
[Name]

5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE
[CAS]

32014-70-3
[Synonyms]

4,5-DIAMINO-2,6-DIHYDROXYPYRIMIDINE
4,5-DIAMINO-2,6-DIHYDROXYPYRIMIDINE SULFATE
4,5-DIAMINO-2,6-DIHYDROXYPYRIMIDINE SULPHATE
4,5-DIAMINOURACIL SULFATE
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULPHATE
5,6-DIAMINOURACIL
5,6-DIAMINOURACIL SULFATE
bis(5,6-diaminouracil) sulphate
5-6-DIAMINO-2-4-DIHYDROXY-PYRIMIDINE*HEM ISULFATE CR
4,5-Diamino-2,6-dihydropyrimidine
5,6-DIAMINO-2,4-DIHYDROXY-PYRIMIDINE 97%
5,6-DIAMINOURACIL HEMISULFATE/4,5-DIAMINO-2,6-DIHYDROXYPYRIMIDINE HEMISULFATE
4,5-Diamino-2,6-dihydroxypyrimidine sulfate, 5,6-Diamino-2,4-dihydroxypyrimidine sulfate
5,6-Diamino-2,4-dihydroxypyrimidine hemisulfate salt
5,6-Diaminouracil sulfate salt
5,6-Diaminouracil sulfate (for AMILORIDE)
[EINECS(EC#)]

250-899-0
[Molecular Formula]

C4H8N4O6S
[MDL Number]

MFCD00135845
[Molecular Weight]

240.19
[MOL File]

32014-70-3.mol
Chemical PropertiesBack Directory
[Melting point ]

>260 °C (dec.)(lit.)
[BRN ]

3781587
[CAS DataBase Reference]

32014-70-3(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[RTECS ]

YQ9625000
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Sodium nitrite-->Ammonium hydroxide-->Urea-->1,4-Dioxane-->Ethyl cyanoacetate-->Sodium dithionite
Spectrum DetailBack Directory
[Spectrum Detail]

5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE(32014-70-3)MS
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE(32014-70-3)IR1
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE(32014-70-3)IR2
5,6-DIAMINO-2,4-DIHYDROXYPYRIMIDINE SULFATE(32014-70-3)Raman
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

32014-70-3(sigmaaldrich)
Hazard InformationBack Directory
[Purification Methods]

The salt is quite insoluble in H2O but can be converted to the free base which is recrystallised from H2O and converted to the sulfate by addition of the required amount of H2SO4. The hydrochloride has m 300-305o(dec) and can be used to prepare the sulfate by addition of H2SO4; it is more soluble than the sulfate. The perchlorate has m 252-254o. The free base has max at 260nm (log 4.24) in 0.1M HCl. [Bogert & Davidson J Am Chem Soc 86 1668 1933, Bredereck et al. Chem Ber 86 850 1953, Sherman & Taylor Org Synth Coll Vol IV 247 1963, Barlin & Pfleiderer J Chem Soc (B) 1425 1971, Beilstein 25 II 382.]
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