ChemicalBook--->CAS DataBase List--->66671-82-7

66671-82-7

66671-82-7 Structure

66671-82-7 Structure
IdentificationMore
[Name]

2,5-Diaminoanisole sulfate
[CAS]

66671-82-7
[Synonyms]

2,5-DIAMINOANISOLE SULFATE
2-Methoxybenzene-1,4-diamine sulphate
2-methoxy-1,4-benzenediaminesulfate
2-Methoxy-1,4-phenylenediaminesulfate
2-methoxy-p-phenylenediaminesulfate
2-methoxy-p-phenylenediaminsulfate
4-benzenediamine,2-methoxy-sulfate(1:1)
4-benzenediamine, 2-methoxy-sulfate
[EINECS(EC#)]

266-443-9
[Molecular Formula]

C7H12N2O5S
[MDL Number]

MFCD00013114
[Molecular Weight]

236.25
[MOL File]

66671-82-7.mol
Chemical PropertiesBack Directory
[CAS DataBase Reference]

66671-82-7(CAS DataBase Reference)
[EPA Substance Registry System]

66671-82-7(EPA Substance)
Safety DataBack Directory
[RIDADR ]

2811
[HazardClass ]

6.1(b)
[PackingGroup ]

III
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Iron-->Dimethyl ether-->N-(4-AMINO-2-METHOXYPHENYL)ACETAMIDE
[Preparation Products]

phanquone
Hazard InformationBack Directory
[Chemical Properties]

Appearance is dark gray to dark brown solid.

[Uses]

2,5-Diaminoanisole sulfate is cyclized with glycerol in the presence of iodine and potassium iodide to generate 6-methoxy-4,7-phenanthroline. Further oxidation can obtain 4,7-phenanthroline-5,6-diquinone, which is an anti-amebic dysentery and bacillary dysentery drug, and can also be used in hair dyes and organic pigment intermediates.

[Synthesis]

The o-acetamido methyl ether is nitrated with nitric acid and reduced with iron powder to obtain 5-amino-2-acetamidoanisole, and then heated to reflux with sulfuric acid at 100-104°C for 0.5h, and hydrolyzed to obtain 2,5-Diaminoanisole sulfate.
Spectrum DetailBack Directory
[Spectrum Detail]

2,5-Diaminoanisole sulfate(66671-82-7)MS
2,5-Diaminoanisole sulfate(66671-82-7)IR1
2,5-Diaminoanisole sulfate(66671-82-7)IR2
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