2-(2,4-ジニトロベンジル)ピリジン
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- CAS番号.
- 1151-97-9
- 化学名:
- 2-(2,4-ジニトロベンジル)ピリジン
- 别名:
- 2-(2,4-ジニトロベンジル)ピリジン;1-[(2-ピリジニル)メチル]-2,4-ジニトロベンゼン;2-[(2,4-ジニトロフェニル)メチル]ピリジン;2(2,4ジニトロベンジル)ピリジン
- 英語名:
- 2-(2,4-Dinitrobenzyl)pyridine
- 英語别名:
- AKOS 92219;TIMTEC-BB SBB003093;2-(2,4-DINITROBENZYL)PYRIDINE;2-(2,4-BISNITROBENZYL)PYRIDINE;2-(2,4-Dinitrobenzyl)pyridine >2-(2,4-Dinitrobenzyl)pyridine,99%;2-[(2,4-dinitrophenyl)methyl]-pyridin;2-[(2,4-dinitrophenyl)methyl]pyridine;Pyridine, 2-[(2,4-dinitrophenyl)Methyl]-;2-ACETYL-5-CHLORO-167-METHYLTHIANAPHTHENE
- CBNumber:
- CB2343620
- 化学式:
- C12H9N3O4
- 分子量:
- 259.22
- MOL File:
- 1151-97-9.mol
- MSDS File:
- SDS
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2-(2,4-ジニトロベンジル)ピリジン 物理性質
2-(2,4-ジニトロベンジル)ピリジン 価格
もっと(3)
メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
東京化成工業
|
D1095 |
2-(2,4-ジニトロベンジル)ピリジン >98.0%(HPLC)
2-(2,4-Dinitrobenzyl)pyridine
>98.0%(HPLC) |
1151-97-9 |
1g |
¥3300 |
2024-03-01 |
購入 |
東京化成工業
|
D1095 |
2-(2,4-ジニトロベンジル)ピリジン >98.0%(HPLC)
2-(2,4-Dinitrobenzyl)pyridine
>98.0%(HPLC) |
1151-97-9 |
5g |
¥10300 |
2024-03-01 |
購入 |
Sigma-Aldrich Japan
|
S765163 |
AldrichCPR
2-(2,4-DINITROBENZYL)PYRIDINE AldrichCPR |
1151-97-9 |
50mg |
¥24400 |
2024-03-01 |
購入 |
2-(2,4-ジニトロベンジル)ピリジン 化学特性,用途語,生産方法
外観
白色~黄色~緑色粉末~結晶
化学的特性
White to Yellow to Green powder to crystal.
使用
2-(2,4-Dinitrobenzyl)pyridine can be used in organic synthesis and pharmaceutical intermediates.
製造方法
Synthesis of 2-(2,4-Dinitrobenzyl)pyridine
A solution of sulfuric acid (15 mL) is placed in an ice bath along with a magnetic stirrer.Benzylpyridine (2.4 mL) is added dropwise, maintaining a temperature below 10°C. This process is then repeated for fuming nitric acid (3.0 mL), once again maintaining the temperature. After addition mixture is allowed to stand at room temperature for 30minutes. Once completed reaction mixture is heated in an 80°C water bath for 20 minutes. Mixture is then poured into a conical flask containing crushed ice (50 cm3) which is stirred in an ice bath. Using a separating funnel aqueous ammonia is added (50 – 100 mL) until the pH rises to ~9 – 10 and filter using a Buchner funnel. Ethyl acetate (40mL) & sodium hydroxide (40mL) is added to the solid and stirred using a magnetic stirrer until dissolved.
Dry the organic layer using magnesium sulfate as the drying agent which is then followed by a rotary evaporator (40°C, vacuum). Product is then washed using cold methylated spirit and left to recrystalise.
2-(2,4-ジニトロベンジル)ピリジン 上流と下流の製品情報
原材料
準備製品
2-(2,4-ジニトロベンジル)ピリジン 生産企業
Global( 73)Suppliers
2-(2,4-ジニトロベンジル)ピリジン スペクトルデータ(13CNMR、IR1、IR2、MS)
1151-97-9(2-(2,4-ジニトロベンジル)ピリジン)キーワード:
- 1151-97-9
- 2-[(2,4-dinitrophenyl)methyl]-pyridin
- TIMTEC-BB SBB003093
- 2-(2,4-DINITROBENZYL)PYRIDINE
- 2-(2,4-BISNITROBENZYL)PYRIDINE
- 2-[(2,4-dinitrophenyl)methyl]pyridine
- 2-(2,4-Dinitrobenzyl)pyridine,99%
- AKOS 92219
- Pyridine, 2-[(2,4-dinitrophenyl)Methyl]-
- 2-(2,4-Dinitrobenzyl)pyridine >
- 2-ACETYL-5-CHLORO-167-METHYLTHIANAPHTHENE
- 2-(2,4-ジニトロベンジル)ピリジン
- 1-[(2-ピリジニル)メチル]-2,4-ジニトロベンゼン
- 2-[(2,4-ジニトロフェニル)メチル]ピリジン
- 2(2,4ジニトロベンジル)ピリジン