tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate
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tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate 속성
- 끓는 점
- 317.9±11.0 °C(Predicted)
- 밀도
- 1.08±0.1 g/cm3(Predicted)
- 산도 계수 (pKa)
- 12.42±0.40(Predicted)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate C화학적 특성, 용도, 생산
Synthesis
To a stirred solution of methyl (1R,3R)-3-((tert-butoxycarbonyl)amino)cyclobutane-1-carboxylate (1.0 g, 4.4 mmol) in THF (20 mL) was added 3M lithium borohydride (9 mL, 9 mmol) at 0° C. Then the reaction mixture was heated and stirred at 60° C for 3 h. The reaction mixture was then transferred into dilute NaOH and the resulting mixture was extracted using ethyl acetate (3×50 mL). The combined organic layer was dried over anhydrous sodium sulfate and filtered. The filtrate was evaporated under reduced pressure and the crude product was purified using silica gel column chromatography (3% MeOH-DCM) to give tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate as a white solid (0.8 g, 91%).tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate 준비 용품 및 원자재
원자재
준비 용품
tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate 공급 업체
글로벌( 53)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Chongqing Chemdad Co., Ltd | +86-023-61398051 +8613650506873 |
sales@chemdad.com | China | 39916 | 58 |
Alchem Pharmtech,Inc. | 8485655694 |
sales@alchempharmtech.com | United States | 63711 | 58 |
Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 |
contact@fuxinpharm.com | China | 10297 | 58 |
Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 |
joe@yuhengpharm.com | CHINA | 21149 | 58 |
Career Henan Chemica Co | +86-0371-86658258 15093356674; |
laboratory@coreychem.com | China | 30255 | 58 |
Shanghai Gubang New Materail Technology Co. LTD | 21-51317962 +8618721305404 |
16728589@qq.com | CHINA | 272 | 58 |
Hefei Hirisun Pharmatech Co., Ltd | +8615056975894 |
shawn@hirisunpharm.com | CHINA | 9923 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | 0551-65418684 +8618949823763 |
sales@tnjchem.com | China | 25363 | 58 |
LEAPCHEM CO., LTD. | +86-852-30606658 |
market18@leapchem.com | China | 43348 | 58 |
Aladdin Scientific | +1-833-552-7181 |
sales@aladdinsci.com | United States | 57511 | 58 |
tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate 관련 검색:
6-bromo-pyridine-2-carboxylic acid tert-butyl ester
Ethylenediaminetetraacetic acid
BOC-TRANS-1,3-AMINOCYCLOHEXANE CARBOXYLIC ACID
ZBC
tert-Butyl (trans-3-(hydroxymethyl)cyclobutyl)carbamate
TRANS-3-(TERT-BUTOXYCARBONYLAMINO)CYCLOBUTANECARBOXYLIC ACID
3-[(TERT-BUTOXYCARBONYL)AMINO]BICYCLO[1.1.1]PENTANE-1-CARBOXYLIC ACID