119-58-4

4,4'-二(N,N-二甲氨基)二苯基甲醇(119-58-4)红外图谱(IR2)

产品名称:4,4'-二(N,N-二甲氨基)二苯基甲醇

CAS:119-58-4

分子式:C17H22N2O

分子量: 270.37

InChI:InChI=1S/C17H22N2O/c1-18(2)15-9-5-13(6-10-15)17(20)14-7-11-16(12-8-14)19(3)4/h5-12,17,20H,1-4H3

InChIKey: YLZSIUVOIFJGQZ-UHFFFAOYSA-N

Smiles:C(O)(C1C=CC(N(C)C)=CC=1)C1C=CC(N(C)C)=CC=1

Mass

MS-NW-7036          
bis(p-dimethylaminophenyl)methanol
C17H22N2O           (Mass of molecular ion:    270)

   Source Temperature: 190 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      15.0       3.0
      18.0       3.4
      27.0       1.2
      28.0       1.6
      39.0       4.1
      41.0       1.5
      42.0      15.6
      43.0       1.6
      44.0       4.2
      50.0       2.6
      51.0       4.7
      52.0       1.9
      53.0       1.2
      63.0       3.6
      64.0       1.4
      65.0       3.5
      66.0       2.1
      68.0       1.0
      75.0       1.9
      76.0       3.5
      77.0      13.9
      78.0       7.1
      79.0       6.9
      80.0       1.5
      89.0       1.6
      90.0       2.2
      91.0       6.2
      92.0       2.4
      93.0       1.5
      96.5       1.0
     102.0       1.0
     103.0       1.7
     103.5       1.5
     104.0       8.1
     105.0       8.9
     106.0       4.5
     107.0       7.5
     110.0       1.0
     115.0       1.8
     117.0       1.6
     118.0      12.4
     118.5       1.6
     119.0       8.6
     119.5       1.0
     120.0      18.9
     121.0      13.5
     122.0      38.4
     123.0       3.9
     125.0       1.0
     126.0       7.4
     126.5       2.9
     127.0       2.6
     132.0       5.5
     133.0       2.6
     134.0      10.7
     135.0       4.1
     139.0       1.1
     140.0       1.1
     148.0      52.6
     149.0       7.7
     150.0      11.3
     151.0       2.1
     152.0       2.6
     153.0       1.8
     163.0       1.0
     164.0       1.1
     165.0       7.7
     166.0       3.1
     167.0       1.4
     179.0       1.0
     180.0       1.0
     181.0       1.0
     192.0       1.3
     193.0       1.6
     194.0       2.8
     195.0       1.2
     196.0       1.3
     197.0       1.1
     208.0       3.0
     209.0       3.2
     210.0      10.1
     211.0       1.9
     221.0       2.4
     223.0       2.0
     224.0       5.3
     225.0       1.6
     226.0       1.6
     237.0      18.8
     238.0       5.3
     239.0       3.0
     240.0       1.7
     251.0       3.0
     252.0       1.7
     253.0     100.0
     254.0      46.1
     255.0       6.8
     267.0       3.1
     268.0      12.3
     269.0      13.2
     270.0      67.1
     271.0      13.4
     272.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₂₂ N₂ O	0.042 g : 0.5 ml CDCl₃
bis(p-dimethylaminophenyl)methanol

    Assign.     Shift(ppm)

      A             7.218
      B             6.673
      C             5.261
      D             3.02
      E             2.893

     Hz     ppm     Int.

   2889.28   7.230    138
   2887.33   7.225     49
   2882.32   7.213     51
   2880.49   7.208    153
   2878.91   7.204     43
   2672.97   6.689     47
   2670.65   6.683    166
   2668.70   6.678     54
   2666.02   6.671     21
   2663.94   6.666     78
   2661.87   6.661    151
   2103.03   5.263     73
   1208.74   3.025    136
   1156.37   2.894   1000
   1148.80   2.875     21

in CDCl3