ChemicalBook
English   Japanese   Germany   Korea
返回ChemicalBook首页>CAS数据库列表>1984-59-4更多图谱> 2,3-二氯茴香醚(1984-59-4)质谱(MS)

1984-59-4

2,3-二氯茴香醚(1984-59-4)质谱(MS)

产品名称:2,3-二氯茴香醚

CAS:1984-59-4

分子式:C7H6Cl2O

分子量: 177.03

InChI:InChI=1S/C7H6Cl2O/c1-10-6-4-2-3-5(8)7(6)9/h2-4H,1H3

InChIKey: HFEASCCDHUVYKU-UHFFFAOYSA-N

Smiles:C1(Cl)=CC=CC(OC)=C1Cl

  • 图谱
    Mass

    MS-NW-6549          
    2,3-dichloroanisole
    C7H6Cl2O            (Mass of molecular ion:    176)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       2.8
          28.0       1.3
          29.0       1.4
          36.0       1.5
          37.0       4.1
          38.0       1.8
          39.0       2.3
          48.0       1.0
          49.0       2.2
          50.0       4.1
          51.0       2.4
          61.0       3.7
          62.0       6.3
          63.0      16.2
          64.0       1.0
          72.0       4.7
          73.0       8.3
          74.0       7.0
          75.0       9.4
          76.0       2.4
          77.0       5.9
          83.0       2.5
          84.0       3.0
          85.0       2.4
          86.0       1.2
          87.0       1.2
          97.0       4.9
          98.0       3.9
          99.0       1.9
         100.0       1.2
         107.0       4.4
         109.0       6.3
         110.0       2.3
         111.0       8.8
         112.0       2.6
         113.0       5.5
         115.0       1.3
         126.0       5.3
         128.0       1.9
         133.0      51.1
         134.0       3.4
         135.0      33.0
         136.0       2.0
         137.0       5.5
         141.0       2.7
         145.0       2.9
         146.0      13.7
         147.0       4.0
         148.0       8.9
         149.0       1.7
         150.0       1.6
         161.0      33.5
         162.0       2.6
         163.0      21.3
         164.0       1.6
         165.0       3.6
         176.0     100.0
         177.0       8.4
         178.0      64.4
         179.0       5.4
         180.0      10.7
         181.0       1.0
    

90 MHz in CDCl3

  • 图谱

    1H NMR 89.56 MHz
    C7 H6 Cl2 O 0.041 g : 0.5 ml CDCl3
    2,3-dichloroanisole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.13 B 7.06 C 6.828 D 3.893 J(A,B)=8.1HZ. J(A,C)=7.0HZ. J(B,C)=2.7HZ.

         Hz     ppm     Int.
    

        649.19   7.249     33
        642.13   7.170     27
        641.13   7.159    127
        635.50   7.096    158
        634.06   7.080    248
        632.81   7.066    250
        627.44   7.006     65
        615.31   6.871     93
        612.63   6.841     66
        608.31   6.793     51
        605.56   6.762     46
        348.69   3.894   1000
    

in CDCl3

  • 图谱

KBr disc

  • 图谱

nujol mull

  • 图谱

  • 图谱

×