41295-20-9

4-氨基-4'-甲基二苯基醚(41295-20-9)红外图谱(IR1)

产品名称:4-氨基-4'-甲基二苯基醚

CAS:41295-20-9

分子式:C13H13NO

分子量: 199.25

InChI:InChI=1S/C13H13NO/c1-10-2-6-12(7-3-10)15-13-8-4-11(14)5-9-13/h2-9H,14H2,1H3

InChIKey: VPCGOYHSWIYEMO-UHFFFAOYSA-N

Smiles:C1(N)=CC=C(OC2=CC=C(C)C=C2)C=C1

Mass

MS-NW-7706          
p-(p-tolyloxy)aniline
C13H13NO            (Mass of molecular ion:    199)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       1.5
      28.0       1.5
      39.0       6.3
      41.0       1.8
      50.0       1.2
      51.0       2.6
      52.0       2.6
      53.0       4.0
      54.0       1.2
      63.0       3.1
      64.0       1.5
      65.0      12.3
      66.0       1.4
      77.0       1.9
      79.0       1.1
      80.0      10.0
      81.0       1.0
      89.0       2.0
      90.0       1.0
      91.0       7.7
      92.0       3.9
      93.0       1.2
     107.0       1.3
     108.0      57.1
     109.0       6.1
     119.0       1.0
     128.0       1.4
     143.0       1.3
     156.0       5.4
     170.0       7.2
     171.0       2.0
     198.0       3.2
     199.0     100.0
     200.0      14.8
     201.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₃ N O	0.039 g : 0.5 ml CDCl₃
p-(p-tolyloxy)aniline

    Assign.     Shift(ppm)

      A             7.071
      B             6.84
      C             6.83
      D             6.644
      E             3.5
      F             2.291

     Hz     ppm     Int.

   2833.62   7.091     34
   2832.89   7.089     38
   2830.81   7.084    208
   2830.08   7.082    235
   2822.02   7.062    278
   2821.53   7.061    262
   2741.94   6.861     58
   2738.53   6.853    411
   2736.33   6.847    181
   2734.74   6.843    411
   2732.18   6.837    231
   2729.86   6.831    515
   2728.39   6.827    171
   2726.20   6.822    379
   2723.39   6.815     54
   2662.84   6.663     62
   2659.42   6.655    506
   2657.23   6.649    155
   2652.83   6.638    142
   2650.76   6.633    386
   2647.22   6.624     45
    915.89   2.292   1000

in CDCl3