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645-36-3

氨基乙醛缩二乙醇(645-36-3)核磁图(13CNMR)

分子式:C6H15NO2

分子量: 133.19

InChI:InChI=1S/C6H15NO2/c1-3-8-6(5-7)9-4-2/h6H,3-5,7H2,1-2H3

InChIKey: HJKLEAOXCZIMPI-UHFFFAOYSA-N

Smiles:C(N)C(OCC)OCC

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    Mass

    MS-NW-5112          
    aminoacetaldehyde diethyl acetal
    C6H15NO2            (Mass of molecular ion:    133)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       4.7
          17.0       1.2
          18.0       1.2
          19.0       3.6
          26.0       2.4
          27.0      12.1
          28.0       7.9
          29.0      27.4
          30.0      38.1
          31.0      21.0
          41.0       1.8
          42.0      14.3
          43.0       5.4
          44.0      16.9
          45.0      11.3
          46.0       3.2
          47.0     100.0
          48.0       1.2
          58.0       4.7
          59.0       3.6
          60.0      26.3
          61.0       1.4
          72.0       1.1
          75.0      36.0
          76.0       1.3
          84.0       1.5
          87.0       2.7
          88.0      22.3
          89.0       1.5
         100.0       1.3
         103.0      68.6
         104.0       4.2
    

90 MHz in CDCl3

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    1H NMR 89.56 MHz
    C6 H15 N O2 0.04 ml : 0.5 ml CDCl3
    aminoacetaldehyde diethyl acetal
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.416 B *1 3.68 C *1 3.56 D 2.778 E 1.26 F 1.226 J(B,C)=-9.3HZ J(B,F)=7.0HZ J(C,F)=6.9HZ

         Hz     ppm     Int.
    

        400.81   4.476     67
        395.63   4.418    144
        390.50   4.361     76
        341.56   3.814     54
        339.31   3.789     58
        334.44   3.735     67
        332.13   3.709    173
        331.31   3.700     85
        327.44   3.657     42
        325.00   3.629    214
        324.25   3.621    191
        321.94   3.595     36
        317.25   3.543    183
        314.81   3.516     63
        310.38   3.466     70
        307.88   3.438     58
        251.38   2.807    114
        248.81   2.779     46
        246.31   2.751    112
        116.56   1.302    488
        112.75   1.259    190
        109.56   1.224   1000
        102.50   1.145    411
    

in CDCl3

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liquid film

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