ChemicalBook
English   Japanese   Germany   Korea
返回ChemicalBook首页>CAS数据库列表>97-77-8更多图谱> 二硫化四乙基秋兰姆(97-77-8)核磁图(13CNMR)

97-77-8

二硫化四乙基秋兰姆(97-77-8)核磁图(13CNMR)

分子式:C10H20N2S4

分子量: 296.54

InChI:InChI=1S/C10H20N2S4/c1-5-11(6-2)9(13)15-16-10(14)12(7-3)8-4/h5-8H2,1-4H3

InChIKey: AUZONCFQVSMFAP-UHFFFAOYSA-N

Smiles:N(CC)(CC)C(=S)SSC(=S)N(CC)CC

  • 图谱
    Mass

    MS-NW-0179          
    N,N,N',N'-tetraethylthiuram disulfide
    C10H20N2S4          (Mass of molecular ion:    296)
    

       Source Temperature: 210 °C
       Sample Temperature:   0 °C
       Direct, 75 eV
    

          18.0       3.0
          27.0      11.1
          28.0       7.2
          29.0      24.3
          30.0       1.4
          42.0       6.4
          44.0      31.2
          45.0       1.8
          54.0       1.0
          56.0       5.0
          59.0       4.8
          60.0      36.0
          61.0       3.3
          62.0       1.5
          64.0       2.1
          70.0       1.0
          72.0      15.8
          76.0       2.1
          77.0       8.5
          86.0       5.2
          87.0       1.0
          88.0      55.1
          89.0       2.4
          90.0       2.4
          91.0       1.9
          92.0       1.3
         116.0     100.0
         117.0       6.9
         118.0       4.8
         148.0      24.2
         149.0       4.5
         150.0       2.4
         180.0       1.3
         212.0       1.0
         296.0      17.9
         297.0       2.6
         298.0       3.4
    

90 MHz in CDCl3

  • 图谱

    1H NMR 89.56 MHz
    C10 H20 N2 S4 0.042 g : 0.5 ml CDCl3
    N,N,N',N'-tetraethylthiuram disulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.021 B 1.382 J(A,B)=7.1HZ

         Hz     ppm     Int.
    

        371.25   4.146    158
        364.06   4.065    609
        356.94   3.986    649
        350.00   3.908    194
        130.75   1.460    494
        123.69   1.382   1000
        119.00   1.329     45
        116.50   1.301    432
    

in CDCl3

  • 图谱

KBr disc

  • 图谱

nujol mull

  • 图谱

AG(II) COMPLEX, IN CS2, RT

  • 图谱

×