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ChemicalBook CAS DataBase List 6-Shogaol

6-Shogaol synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: H2 / Raney-Ni / -10 °C
2: (i) nBuLi, iPr2NH, THF, (ii) /BRN= 1209232/
3: TiCl4 / CH2Cl2 / -78 °C
4: TsOH / benzene / Heating

References:

Banno,K.;Mukaiyama,T. [Bulletin of the Chemical Society of Japan,1976,vol. 49,p. 1453 - 1454]

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